200L Double Layer Jacketed Glass Reactor
Description
200L double layer jacketed glass reactor
Product introduction:
This machine has electric constant speed stirring system, condensation and dropping system. The interlayer of kettle body needs to be connected with heating or cooling circulation equipment. When the material is stirred, the circulating hot solution or cooling liquid is injected through the interlayer to make the materials in the kettle are heated or cooled at a constant temperature. When the material is heated and reacted, the evaporation efficiency can be improved under vacuum conditions (a vacuum device need to be connected). The solvent vapor is cooled into liquid when passing through the glass condensing coil (a cooling device need to be connected), which can be refluxed into the kettle. It can also be recycled through the lower valve of the dean-stark. When the reaction is completed, the material can be discharged from the side outlet at the bottom of the kettle.
This series of products need to be equipped with a vacuum device, a high-temperature or low-temperature circulation device to form system devices.
Basic configuration:
• The parts in contact with the material are all made of high borosilicate glass (expansion coefficient 3.3) and PTFE materials, which have stable performance and are not easy to react with the materials.
• Using aluminum alloy + stainless steel material as frame body
• Glass + PTFE discharge valve, side material discharge without effusion.
• Low-speed power-increasing motor, electronic stepless speed regulation, fine adjustment by knob, speed control box with dual display function can digitally display the speed and the temperature of the material in the kettle.
• The stirring system adopts ceramic bearings and mechanical seals to prevent the stirring rod from wearing out.
• Using PT100 temperature sensor, 304 stainless steel material, wrapped by transparent PTFE tube outside , double anti-corrosion.
• Vacuum pressure gauge shows real-time vacuum by pointer.
• Crescent-type stirring paddle, 304 stainless steel + PTFE stirring blade; the material of the stirring rod is 304 stainless steel, and it is wrapped in PTFE tube outside.
• There is a universal wheel with brake at the bottom of the equipment, which can be moved as a whole and be operated conveniently.
• Fuse safety protection
Technical parameter:
| Model | S212-200L | |
| Reactor volume | 200L, inner diameter 600mm, outer diameter 650mm, inner length 840mm | |
| Interlayer volume | About 40L | |
| Voltage/Frequency | 220V 50Hz/110V 60Hz | |
| Stirring motor power | 750W1/5 | |
| Stirring speed | 0-280rpm/min | |
| Temperature range of reactor | -80ºC~+250ºC | |
| Temperature measuring accuracy | ±1ºC | |
| Vacuum | 0.098Mpa | |
Kettle lid | Stirring port | Φ60mm flange port |
| Condensation reflux port | 50# ball mill port | |
| Dropping stark port | 50# ball mill port | |
| Pressure relief port | 34# standard port | |
| Temperature measuring port | Φ45mm flange port | |
| Solid feeding port | Φ80mm flange port, inner diameter Φ60mm matching PTFE cover | |
| Stirring paddle | Φ20×1300H(mm) blade 240mm | |
| Condenser | Φ160mm×600H(mm), lower Φ60mm flange port | |
| Condensing area | 0.95 | |
| Dean-stark | Upper Φ60 flange port, left 50# ball mill stopper, right 24# standard port with multi-function valve, lower 50#ball mill plug valve | |
| Dropping flask | 5L barrel shape, upper 29#standard port with air releasing valve×2pcs, 34#standard port with glass stopper | |
| Collection flask | 10L, upper 50#ball mill port, 24#standard port with air releasing valve×2pcs, lower glass material releasing valve | |
| Pressure relief valve | 34#standard plug valve, releasing valve (pagoda joint) with 12mm outer diameter | |
| Material discharging port | Φ100mm flange, Φ65mm material discharge hole; oblique discharging port (pagoda joint) Φ40mm; 300mm from the ground | |
| Vacuum nozzle | Pagoda joint with 12mm outer diameter | |
| In and out circulating nozzle of condenser coil | Pagoda joint with 15mm outer diameter | |
| Overall dimension(W*D*H) | 1250×930×2800mm | |
| Net weight | 175KG | |
| Packing dimension | 2200×790×875mm 1385×880×910mm two wooden packages 2.63m³ | |
| Packing weight | 271(159+112)KG | |
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